Semiautomated Identification of the Phase Diagram for Enantiotropic Crystallizations using ATR-FTIR Spectroscopy and Laser Backscattering
نویسندگان
چکیده
UniVersity of Illinois at Urbana-Champaign, 600 South Mathews AVenue, Urbana, Illinois 61801, United States of America; Department of Chemical and Biomolecular Engineering, National UniVersity of Singapore, 4 Engineering DriVe 4, Singapore 117576; Institute of Chemical and Engineering Sciences, 1 Pesek Road, Jurong Island, Singapore 627833; and Department of Chemical Engineering, Massachusetts Institute of Technology, 77 Massachusetts AVenue, Cambridge, Massachusetts 02139, United States of America
منابع مشابه
Selective Crystallization of the Metastable Anhydrate Form in the Enantiotropic Pseudo-Dimorph System of l-Phenylalanine using Concentration Feedback Control
A batch recipe for the selective crystallization of the metastable anhydrate form of an enantiotropic pseudo-dimorph system, L-phenylalanine, in a mixed solvent system (75 wt % water and 25 wt % 2-propanol) was implemented by controlled tracking of a designed trajectory in the phase diagram. The solubility curves of both the anhydrate and monohydrate forms were determined using attenuated total...
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